Characterization of the particles surface of dried dairy products
Abstract
During production or storage of dehydrated dairy products, milk constituents may undergo redistribution, resulting in heterogeneity between the surface and its interior. The main objective of this work was to map the surfaces of different dehydrated dairy products, with the combined use of Raman spectroscopy and scanning electron microscopy (SEM) coupled with energy dispersive spectroscopy (EDS). It was intended to characterize the surfaces of the particles of interest in both instruments and to perform the mapping of these, within specific populations. The proposal to combine different techniques aimed, in addition to obtaining complementary data, to show that it is possible to advance in the research of dairy products when analyzing the particles under different analytical perspectives. All analyzes were carried out from industrialized products with lots, manufacture and validity dates monitored. From the spectroscopic profiles of the particles, it was possible to verify differences when the set of particles was analyzed, as well the target particles alone. It was possible to perform the characterization of the particles using different analytical techniques providing a data set that expands information about the particles of the dairy powders analyzed.
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ALMEIDA, M. R.; STEPHANI, R.; OLIVEIRA, L. F. C. Fourier-transform Raman analysis of milk powder: A potential method for rapid quality screening. Journal of Raman Spectroscopy, v. 42, n. 7, p. 1548-1552, 2011.
CARVALHO, A. F.; MARTINS, E.; RODRIGUES, R. C.; SCHUCK, P.; PERRONE, I. T. Tecnologia de lácteos concentrados e desidratados: O estado da arte da microbiologia de processo. Indústria de Laticínios, n. 121, p. 71-73, 2016.
DENECKERE, A. Development, optimization and application of Raman spectroscopic and X-ray fluorescence spectroscopic methodology in the field of cultural heritage. 2012. Dissertation (Doctor Ph.D. in Sciences, Chemistry) – Faculty of Sciences, Ghent University, Gent, 2012.
EVANS, A. A.; CHEUNG, E.; NYBERG, K. D.; ROWAT, A. C. Wrinkling of milk skin is mediated by evaporation. Soft Matter, v. 13, p. 1.056-1.062, 2017.
KIM, E. H. J.; CHEN, X. D.; PEARCE, D. Surface composition of industrial spray-dried milk powders. Effects of spray drying conditions on the surface composition. Journal of Food Engineering, v. 94, p. 169-181, 2009.
MAZUREK, S.; SZOSTAK, R.; CZAJA, T.; ZACHWIEJA, A. Analysis of milk by FT-Raman spectroscopy. Talanta, v. 138, p. 285-289,2015.
MURRIETA-PAZOS, I.; GAIANI, C.; GALET, L.; SCHER, J. Composition gradient from surface to core in dairy powders: Agglomeration effect. Food Hydrocolloids, v. 26, n.1, p. 149-158, 2012.
SILVA, P. H. F. Leite: aspectos de composição e propriedades. Química Nova na Escola, v. 6, p.3-5, 1997.
SIMEÃO, M; SILVA, C. R.; STEPHANI, R.; OLIVEIRA, L. F. C.; SCHUCK, P.; CARVALHO, A. F.; PERRONE, I T. Lactose crystallisation in concentrated whey: The influence of vat type. International Journal of Dairy Technology, v. 71, n. 2, p. 478-483, 2018.
STAHL, T.; FALK, S.; ROHRBECK, A.; GEORGII, S.; HERZOG, C.; WIEGAND, A.; HOTZ, S.; BOSCHEK, B., ZORN, H.; BRUNN, H. Migration of aluminum from food contact materials to food - a health risk for consumers? Part I of III: Exposure to aluminum, release of aluminum, tolerable weekly intake (TWI), toxicological effects of aluminum, study design, and methods. Environmental Sciences Europe, v. 29, n. 19, p. 1-8, 2017.
STEPHANI, R.; OLIVEIRA, K. S.; ALMEIDA, C. E. R.; PERRONE, I. T.; CARVALHO, A. F.; OLIVEIRA, L. F. C.; ALMEIDA, M. R. Raman spectroscopy as a tool to identify modification of whey protein concentrate (WPC) during shelf life. Food Packaging and Shelf Life, v. 11, p. 1-9, 2017.
WIEBOLDT, D. Understanding Raman spectrometer parameters. Spectroscopy, special issue, 2010. Disponível em: http://www.spectroscopyonline.com/understanding-raman-spectrometer-parameters?id=&pageID=1&sk=&date=
YANG, S.; AKKUS, O.; CREASEY, D. 1064-nm Raman: The right choice for biological samples? Spectroscopy, v. 32, n.6, p. 46-54, 2017.
ZHONG, Y.; WU, Y.; ZHENG, Y.; ZHU, H.; LIU, Z.; JIAO, S. Assessment of radio frequency heating on composition, microstructure, flowability and rehydration characteristics of milk powder. Food Science and Technology, v. 37, n. 4, p. 544-551, 2017.
ZHOU, G.; SUN, S. Q.; YU, L.; XU, C. H.; NODA, I.; ZHANG, X. R. Sequential changes of main components in different kinds of milk powders using two-dimensional infrared correlation analisys. Journal of Molecular Structure, v. 799, n. 6, p. 77-84, 2006.
DOI: https://doi.org/10.14295/2238-6416.v75i1.755
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